2,9-二(3-戊烷基)异喹啉并[4',5',6':6,5,10]蒽并[2,1,9-def]异喹啉-1,3,8,10(2H,9H)-四酮合成路线 （共 3 条）
→
110590-81-32,9-二(3-戊烷基)异喹啉并[4',5',6':6,5,10]蒽并[2,1,9-def]异喹啉-1,3,8,10(2H,9H)-四酮
反应条件
1H-imidazole T=200°C; 2 h;
参考文献
Yang, Yang; Wang, Yaochuan; Xie, Yuanpeng; Xiong, Tao; Yuan, Zhongyi; Zhang, Youdi; Qian, Shixiong; Xiao, Yi
Chemical Communications, 2011 , vol. 47, # 38 p. 10749 - 10751
→
110590-81-32,9-二(3-戊烷基)异喹啉并[4',5',6':6,5,10]蒽并[2,1,9-def]异喹啉-1,3,8,10(2H,9H)-四酮
反应条件
1: sodium-dihydrobis(2-methoxyethoxy)aluminate / toluene / 4 h / 140 °C 2: 46 percent / imidazole / 4 h / 160 °C View Scheme
参考文献
Demming, Stefan; Langhals, Heinz
Chemische Berichte, 1988 , vol. 121, p. 225 - 230
110590-81-32,9-二(3-戊烷基)异喹啉并[4',5',6':6,5,10]蒽并[2,1,9-def]异喹啉-1,3,8,10(2H,9H)-四酮
→
反应条件
potassium hydroxide in tert-butyl alcohol 0.5 h; Heating; Title compound not separated from byproducts.;
参考文献
Percec, Virgil; Aqad, Emad; Peterca, Mihai; Imam, Mohammad R.; Glodde, Martin; Bera, Tusha K.; Miura, Yoshiko; Balagurusamy, Venkatachalapathy S. K.; Ewbank, Paul C.; Wuerthner, Frank; Heiney, Paul A.
Chemistry - A European Journal, 2007 , vol. 13, # 12 p. 3330 - 3345
