反应条件
1: (Z)-2,3,3-trifluoro-1-iodoprop-1-ene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 0.5 h;
2: With ZnCl2*TMEDA in tetrahydrofuran; hexane
T=-78 - 20°C; 0.75 h;
3: 1-chloro-4-iodobenzene With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; hexane
T=60°C; 4 h;
参考文献
Konno, Tsutomu; Chae, Jungha; Kanda, Masashi; Nagai, Go; Tamura, Kazushige; Ishihara, Takashi; Yamanaka, Hiroki
Tetrahedron, 2003 , vol. 59, # 38 p. 7571 - 7580