反应条件
1.1: 93 percent / NaBH4; CeCl3*7H2O / ethanol / 1 h / 0 °C 2.1: n-Bu3SnH; AIBN / toluene / 2.5 h / 80 °C 2.2: 71 percent / I2 / CH2Cl2 / 0.17 h / 25 °C 3.1: AsPh3 / Pd2(dba)3 / 1-methyl-pyrrolidin-2-one / 0.17 h 3.2: 67 percent / 1-methyl-pyrrolidin-2-one / 3 h / 30 °C 4.1: Dess-Martin periodinane; pyridne / CH2Cl2 / 1.5 h / 25 °C View Scheme
参考文献
Dominguez, Marta; Alvarez, Rosana; Martras, Silvia; Farres, Jaume; Pares, Xavier; De Lera, Angel R.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 22 p. 3368 - 3373
