反应条件
in neat (no solvent) byproducts: propylene; under Ar; mixt. of Ti complex and n-propyl iodide stirred at 20°Cfor several minutes, stored for 24 h; soln. concd., stored at 20°C under Ar for 3 d, crystals sepd. by decantation, dried at 20°C for 2 h under vac., soln. evapd. undervac. to dryness, residue extd. with n-hexane; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 4 p. 557 - 565
