1: NaBH4 / ethanol / 0.5 h / 0 - 5 °C
2: 68.4 percent / 50percent aq. NaOH / tetrabutylammonium bromide / benzene / 5 h / Ambient temperature
View Scheme
参考文献
Ivanov, P. Yu.; Alekseeva, L. M.; Bokanov, A. I.; Shvedov, V. I.; Sheinker, Yu. N.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 1 p. 62 - 65
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 1 p. 71 - 75
With thionyl chloride in N,N-dimethyl-formamide; benzene T=50 - 55°C; 2 h;
参考文献
Ivanov, P. Yu.; Alekseeva, L. M.; Bokanov, A. I.; Shvedov, V. I.; Sheinker, Yu. N. Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 1 p. 62 - 65Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 1 p. 71 - 75
With sodium tetrahydroborate in ethanol T=0 - 5°C; 0.5 h;
参考文献
Ivanov, P. Yu.; Alekseeva, L. M.; Bokanov, A. I.; Shvedov, V. I.; Sheinker, Yu. N. Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 1 p. 62 - 65Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 1 p. 71 - 75
