sodium hydroxide; tetrabutylammomium bromide in benzene
5 h; Ambient temperature;
参考文献
Ivanov, P. Yu.; Alekseeva, L. M.; Bokanov, A. I.; Shvedov, V. I.; Sheinker, Yu. N.
Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 1 p. 62 - 65
Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 1 p. 71 - 75
With sodium tetrahydroborate in ethanol T=0 - 5°C; 0.5 h;
参考文献
Ivanov, P. Yu.; Alekseeva, L. M.; Bokanov, A. I.; Shvedov, V. I.; Sheinker, Yu. N. Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 1 p. 62 - 65Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 1 p. 71 - 75
Multi-step reaction with 2 steps 1: 81.7 percent / SOCl2 / dimethylformamide; benzene / 2 h / 50 - 55 °C2: NaBH4 / ethanol / 0.5 h / 0 - 5 °C
参考文献
Ivanov, P. Yu.; Alekseeva, L. M.; Bokanov, A. I.; Shvedov, V. I.; Sheinker, Yu. N. Pharmaceutical Chemistry Journal, 1987 , vol. 21, # 1 p. 62 - 65Khimiko-Farmatsevticheskii Zhurnal, 1987 , vol. 21, # 1 p. 71 - 75
