反应条件
in methanol addn. of acid in anhyd. methanol to slight excess of Tl2CO3, refluxing and stirring (several h); filtn. excess of Tl2CO3, concn. and pptn. by addn. of ethyl ether. Recrystn. from abs. ethanol, vac.-dried. Purity 99.7 mol-percent (d.s.c.);
参考文献
Labban, A. K.; Fuente, F. L. Lopez de la; Cheda, J. A. R.; Westrum, Edgar F.; Fernandez-Martin, F.
Journal of Chemical Thermodynamics, 1989 , vol. 21, # 4 p. 375 - 384