1: 1-bromo-hexane With pyrene; zinc in N,N-dimethyl-formamide T=20°C; 1 h; 2: 4'-iodoacetophenone With bis (triortho-tolylphosphine)palladium(II) chloride in tetrahydrofuran; N,N-dimethyl-formamide T=70°C; 3 h;
1: With potassium carbonate in butanone Heating; 2: With potassium hydroxide in ethanol; water 0.5 h; Heating; 3: With hydrogenchloride in water 3 h; Heating;
参考文献
Tokushige; Mihara; Koide
Molecular Crystals and Liquid Crystals, 2004 , vol. 414, p. 27 - 38
tri[2-(2-methoxyethoxy)ethyl]amine in chlorobenzene T=100°C; 0.25 h; various tris(polyoxaalkyl)amines as phase-transfer catalysts, other alkyl and aryl halides, other sodium salts; Product distribution;
参考文献
Soula, Gerard
Journal of Organic Chemistry, 1985 , vol. 50, # 20 p. 3717 - 3721
