反应条件
Multi-step reaction with 4 steps 1.1: acetonitrile / 24 h / 90 °C / Inert atmosphere2.1: potassium hexamethylsilazane / tetrahydrofuran / 2 h / -78 - 20 °C / Inert atmosphere3.1: (R,R)-3,5-diethylphenylTADDOLPPh; Pt(dibenzylideneacetone)3 / tetrahydrofuran / 0.33 h / 80 °C / Inert atmosphere3.2: 20 - 60 °C / Inert atmosphere3.3: 0 - 20 °C / Inert atmosphere4.1: toluene-4-sulfonic acid / 0.5 h / 60 °C / Inert atmosphere
参考文献
Kliman, Laura T.; Mlynarski, Scott N.; Ferris, Grace E.; Morken, James P. Angewandte Chemie - International Edition, 2012 , vol. 51, # 2 p. 521 - 524
