in neat (no solvent)
Irradiation (UV/VIS); irradiation of a 1:2 molar mixt. of Mn complex and amine with UV light in a quartz vessel under Ar, 140h; crystn. of dialkylurea; filtration, refluxing crystals (EtOH), filtration, evapn.; evapn. of mother liquor of first filtration; washing (light petroleum); elem. anal.;
参考文献
Srivastava, S.C.; Shrimal, A.K.; Srivastava, Amar
Journal of Organometallic Chemistry, 1991 , vol. 414, # 1 p. 65 - 69
1: With palladium on aluminium oxyhydroxide in n-heptane
T=90°C; 12 h; Inert atmosphere;
2: With hydrogen in n-heptane
T=25°C; P=760.051 Torr; 6 h;
参考文献
Kwon, Min Serk; Kim, Sungjin; Park, Sungho; Bosco, William; Chidrala, Ravi Kumar; Park, Jaiwook
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2877 - 2879
