反应条件
1: 1.) zinc chips / 1.) THF, 0 deg C, 1 h, 2.) THF, 25 deg C, 1h
2: dimethylsulfoxide / 200 °C
3: 71 percent / lithium amide / liquid ammonia; tetrahydrofuran / 0.75 h
4: 1.) 35percent H2O2, conc. H2SO4, 2.) triethylamine, acetic anhydride / 1.) THF, 20 deg C, 24 h, 2.) 20 deg C, 2 h
5: 71 percent / H2, quinoline / 5percent Pd/C/BaSO4 / hexane
View Scheme
参考文献
Fehr, Charles; Galindo, Jose; Ohloff, Guenther
Helvetica Chimica Acta, 1981 , vol. 64, # 5 p. 1247 - 1256
