N,N'-二甲基-1,3-丙二胺合成路线 （共 33 条）
反应条件
1: With selenium T=20°C; P=750.075 Torr; 2 h; neat (no solvent); 2: With oxygen T=20°C; P=750.075 Torr; 1 h; neat (no solvent);
参考文献
Mizuno, Takumi; Nakai, Takeo; Mihara, Masatoshi
Synthesis, 2010 , # 24 art. no. F15510SS, p. 4251 - 4255
反应条件
hydrogenchloride; sodium hydroxide in water
参考文献
Mitsui Toatsu Chemicals, Inc.
Patent: US4918186 A1, 1990 ;
参考文献
Boon
Journal of the Chemical Society, 1947 , p. 313
Journal of the Chemical Society, 1956 , p. 5041
反应条件
sodium hydroxide in dichloromethane; water T=20°C; 60 h;
参考文献
Iturrospe, Amaia; Artetxe, Benat; Reinoso, Santiago; San Felices, Leire; Vitoria, Pablo; Lezama, Luis; Gutierrez-Zorrilla, Juan M.
Inorganic Chemistry, 2013 , vol. 52, # 6 p. 3084 - 3093
反应条件
potassium hydroxide in methanol Inert atmosphereReflux;
参考文献
Pandiyan, Thangarasu; Guadalupe, Hernandez J.; Cruz, Julian; Bernes, Sylvain; Ugalde-Salvdivar, Victor M.; Gonzalez, Ignacio
European Journal of Inorganic Chemistry, 2008 , # 21 p. 3274 - 3285
反应条件
transamination, boiling under inert atmosphere, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling the educts in an inert atmosphere and in an inert solvent, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
transamination, boiling the educts under nitrogene, distn. of dimethylamine during the reaction; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
N-ethyl-N,N-diisopropylamine; citric acid; palladium monocarbide in tetrahydrofuran; methanol
参考文献
Riken
Patent: US8076299 B2, 2011 ;
反应条件
triethylamine in tetrahydrofuran
参考文献
Riken
Patent: US8076299 B2, 2011 ;
