N,N'-二甲基-1,3-丙二胺合成路线 （共 33 条）
反应条件
triethylamine in benzene
参考文献
Gol'din,G.S. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1971 , vol. 41, p. 2465 - 2468,2492 - 2494
反应条件
in Petroleum ether stoich. amt., under nitrogene;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
反应条件
in benzene
reflux of soln. (5 h);; evapn. of volatiles (vac.); distillation; elem. anal.;;
参考文献
Cragg, R. Harry; Nazeri, Manije
Journal of Organometallic Chemistry, 1986 , vol. 303, p. 329 - 336
反应条件
1: With pyridine
24 h; Heating;
2: With iodine in pyridine
20 h; Heating;
参考文献
Denk, Michael K.; Gupta, Shilpi; Brownie, John; Tajammul, Sabiha; Lough, Alan J.
Chemistry - A European Journal, 2001 , vol. 7, # 20 p. 4477 - 4486
反应条件
1: diethyl ether
2: 91 percent / S8 / 12 h / 150 °C
View Scheme
参考文献
Li, Chau-der; Mella, Sharon L.; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 9 p. 1089 - 1092
反应条件
hydrogenchloride; sodium nitrite
参考文献
Gol'din,G.S. et al.
Journal of Organic Chemistry USSR (English Translation), 1970 , vol. 6, p. 1177 - 1179
Zhurnal Organicheskoi Khimii, 1970 , vol. 6, p. 1171 - 1173
反应条件
triethylamine in benzene
T=20°C; 2 h;
参考文献
Nunez, Andres; Berroteran, Dyanna; Nunez, Oswaldo
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 13 p. 2283 - 2289
反应条件
triethylamine in benzene
0.75 h;
参考文献
Nunez, Andres; Berroteran, Dyanna; Nunez, Oswaldo
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 13 p. 2283 - 2289
反应条件
boiling the educts in an inert solvent under nitrogene; distn.;
参考文献
Gmelin Handbook: B: B-Verb.1, 2.5.1.3, page 122 - 126
