1: With benzotriazol-1-ol; triethylamine in dichloromethane 0.25 h; Cooling with ice; 2: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane T=20°C; Cooling with ice;
D'Alelio; Reid
Journal of the American Chemical Society, 1937 , vol. 59, p. 111
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Trowbridge et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 990,994
in tetrahydrofuran; isopropyl alcohol to soln. of 4-formylphenylboronic acid (6.7 mmol) in THF soln. of diethanolamine (7.3 mmol) in 2-propanol added, stirred for 3h at room temp.; filtered, washed with THF, dried;
参考文献
Mlynarz, Piotr; Rydzewska, Agata; Pokladek, Ziemowit
Journal of Organometallic Chemistry, 2011 , vol. 696, # 2 p. 457 - 460
