1: azacycloheptane With dimethylsulfide borane complex in tetrahydrofuran
T=0°C;
2: With n-butyllithium in tetrahydrofuran; hexane
T=0°C;
3: 2-fluoro-benzonitrile in tetrahydrofuran; hexane
T=65°C; 2 h; Further stages.;
参考文献
Thomas; Collins; Cuzens; Spiciarich; Goralski; Singaram
Journal of Organic Chemistry, 2001 , vol. 66, # 6 p. 1999 - 2004