反应条件
1.1: 98.6 percent / Et3N; 4-dimethylaminopyridine / tetrahydrofuran / 1 h / 0 °C 2.1: LDA / tetrahydrofuran; hexane / 0.5 h / -78 °C 2.2: 85.3 percent / LiI / tetrahydrofuran; hexane; various solvent(s) / 3.5 h / -78 - -30 °C 3.1: 89.6 percent / 2-methyl-2-butene; H2O2; tetrabutylammonium hydroxide / 1,2-dimethoxy-ethane; H2O / 0.17 h / -10 °C 4.1: 94.6 percent / H2 / Pt/C / propan-2-ol / 2.5 h / 3800 Torr View Scheme
参考文献
Hasegawa, Tomoyuki; Kawanaka, Yasufumi; Kasamatsu, Eiji; Iguchi, Yoichi; Yonekawa, Yoshihira; Okamoto, Masaki; Ohta, Chiaki; Hashimoto, Shinsuke; Ohuchida, Shuichi
Organic Process Research and Development, 2003 , vol. 7, # 2 p. 168 - 171
