1: [14C]-Sucrose With di(n-butyl)tin oxide in methanol Heating; 2: octanoic acid chloride With pyridine in N,N-dimethyl-formamide T=20°C; 1.5 h; Further stages.;
1: 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane With sodium in toluene T=110°C; 0.75 - 1.15 h; 2: octanoic acid chloride in toluene T=45 - 60°C; 1 - 2 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 7-9 ;
1: TESPT With sodium in Solventreg; 140 T=110°C; 0.75 h; 2: octanoic acid chloride in Solventreg; 140 T=45 - 104°C; 1 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 9 ;
1: 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane With sodium in toluene T=110°C; 0.75 - 1.15 h; 2: octanoic acid chloride in toluene T=45 - 60°C; 1 - 2 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 7-9 ;
