1: TESPT With sodium in Solventreg; 140 T=110°C; 0.75 h; 2: octanoic acid chloride in Solventreg; 140 T=45 - 104°C; 1 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
参考文献
General Electric Company
Patent: US6777569 B1, 2004 ;
Location in patent: Page column 9 ;
pyridine in dichloromethane 1 h; Ambient temperature;
参考文献
Kocienski, Philip J.; Pelotier, Beatrice; Pons, Jean-Marc; Prideaux, Heather
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 8 p. 1373 - 1382
1: pyridine / CH2Cl2 2: Heating 3: aq. NaBH4 / tetrahydrofuran / 1 h 4: 83 percent / 6 N aq. NaOH / 0.02 h / 110 °C View Scheme
参考文献
Sakai, Ryuichi; Stroh, Justin G.; Sullins, David W.; Rinehart, Kenneth L.
Journal of the American Chemical Society, 1995 , vol. 117, # 13 p. 3734 - 3748
