butane-2-thiol; hydrogen fluoride T=4 - 6°C; P=362.004 Torr; effect of the electrolysis operation and the additive to the side products, investigation of the modified Simons electrolysis process; MechanismProduct distribution;
参考文献
Prokop, H. W.; Zhou, H-J.; Xu, S-Q.; Wu, C-H.; Chuey, S. R.; Liu, C. C.
Journal of Fluorine Chemistry, 1989 , vol. 43, p. 257 - 276
1: 4,4,13,13-tetraethoxy-3,14-dioxa-8,9-dithia-4,13-disilahexadecane With sodium in toluene T=110°C; 0.75 - 1.15 h; 2: octanoic acid chloride in toluene T=45 - 60°C; 1 - 2 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
1: TESPT With sodium in Solventreg; 140 T=110°C; 0.75 h; 2: octanoic acid chloride in Solventreg; 140 T=45 - 104°C; 1 h; 3: With water in toluene T=45°C; Product distribution / selectivity;
