in tetrahydrofuran addn. of Me3SnNa in THF to a soln. of 2-bromooctane in THF at 0°C under Ar; quenching after 1 h with a large excess H2O2, extg. (pentane), washing of extracts (H2O), drying (Na2SO4), GLPC;
参考文献
Journal of the American Chemical Society, , vol. 107, # 2 p. 416 - 423