反应条件
water in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide soln. of Ph2GeK2 in HMPA/THF added to n-C8H17Br, stirred at room temp. for 30 min, cooled with water bath, hydrolyzed; extd. with ether, org. layer dried over anhyd. Na2SO4, isolated by preparative GLC and TLC;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 58, # 5 p. 1443 - 1447
