lithium borohydride; B-OMe-9-borabicyclo[3.3.1]nonane in diethyl ether T=25°C; 1 h; rate of reduction in presence and absence of catalyst (fig.5); Product distribution;
参考文献
Brown, Herbert C.; Narasimhan, S.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3891 - 3898
in further solvent(s) addn. of Me3SnNa in tetraglyme to a soln. of 2-bromooctane in tetraglyme at 0°C under Ar; quenching after 1 h with a large excess H2O2, extg. (pentane), washing of extracts (H2O), drying (Na2SO4), GLPC;
参考文献
Alnajjar, Mikhail S.; Kuivila, Henry G.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 416 - 423
in tetrahydrofuran addn. of Me3SnK in THF to a soln. of 2-bromooctane in THF at 0°Cunder Ar; quenching after 1 h with a large excess H2O2, extg. (pentane), washing of extracts (H2O), drying (Na2SO4), GLPC;
参考文献
Alnajjar, Mikhail S.; Kuivila, Henry G.
Journal of the American Chemical Society, 1985 , vol. 107, # 2 p. 416 - 423
