反应条件
in tetrahydrofuran byproducts: methane, butane; excess MeLi, 30-50°C, ca. 1 h; Li(1+) cation in the resulting complex is solvated with 3-5 molecules of THF, trace of butenes were also detected, U-Me to U-Bu complexes ratio was 9:1 according to (1)H NMR spectral data; GC anal. of the gas. phase, (1)H NMR;
参考文献
Arnaudet, Lucile; Folcher, Gerard; Marquet-Ellis, Hubert; Klaehne, Eberhard; Yuenlue, Kenan; Fischer, R. Dieter
Organometallics, 1983 , vol. 2, p. 344 - 346
