反应条件
1: 1) HAl(i-Bu)2 / 1) pentane, 10-15 deg C, 1 h, 2) ether, pentane, 20 deg C
2: 100 percent / HBr / diethyl ether / 5 h / -78 °C
3: diethyl ether / 24 h / Heating
4: 1) 1,5 N BuLi, 2) H2 / 2) PtO2 / 1) ether, hexane, 0 deg C, 2) 20 deg C, glac. HOAc
View Scheme
参考文献
Bogdanovic, Borislav; Hullen, Albert; Konstantinovic, Stanimir; Krawiecka, Bozena; Mynott, Richard
Chemische Berichte, 1981 , vol. 114, # 6 p. 2261 - 2271
