in tetrahydrofuran
THF, ambient temp., stirring overnight;; evapd. in vac., washed with hexane, dried in vac., crystd. from hexane at -15°C; elem. anal.;;
water; acetic acid; copper(l) chloride
T=30 - 40°C; unter Druck;
参考文献
Gen. Aniline and Film Corp.
Patent: US2273141 , 1938 ;
Full Text Show Details
I.G. Farbenind.
Patent: DE724759 , 1937 ;
DRP/DRBP Org.Chem.
Full Text Show Details
Reppe et al.
Justus Liebigs Annalen der Chemie, 1955 , vol. 596, p. 65
1: dibutylamine With sodium hydroxide in ethanol
0.5 h; Inert atmosphereSchlenk technique;
2: carbon disulfide in ethanol
1 h; Inert atmosphereSchlenk technique;
3: diphenyltin dichloride in ethanol
0.5 h; Inert atmosphereSchlenk technique;
参考文献
Ramasamy, Karthik; Kuznetsov, Vladimir L.; Gopal, Kandasamy; Malik, Mohammad A.; Raftery, James; Edwards, Peter P.; O'Brien, Paul
Chemistry of Materials, 2013 , vol. 25, # 3 p. 266 - 276
