3-(5,5-二甲基-2-氧代-2-[1,3,2]二氧杂磷杂环己基) -4-(3-硝基苯基)-丁-3-烯-2-酮合成路线 （共 5 条）
反应条件
trifluoroacetic acid in toluene 1.) 60 deg C, 30 min, 2.) 0-10 deg C, 3 h;
参考文献
Sakoda; Matsumoto; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2377 - 2381
反应条件
piperidine; acetic acid in benzene 6.5 h; Heating;
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
1: 65.8 percent / diethyl ether / 7 h / Heating 2: 31 percent / piperidine, acetic acid / benzene / 6.5 h / Heating View Scheme
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
1: 33 percent / 100 °C 2: 65.8 percent / diethyl ether / 7 h / Heating 3: 31 percent / piperidine, acetic acid / benzene / 6.5 h / Heating View Scheme
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
in toluene 5 h; Heating;
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
