2-丙酮基-5,5-二甲基-2-氧代-1,3,2-二氧杂磷杂环己烷合成路线 (共 17 条)
反应条件
trifluoroacetic acid in toluene 1.) 60 deg C, 30 min, 2.) 0-10 deg C, 3 h;
参考文献
Sakoda; Matsumoto; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2377 - 2381
反应条件
piperidine; acetic acid in benzene 6.5 h; Heating;
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
chloroacetic acid in toluene 3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
trifluoroacetic acid 1) toluene, 2) r.t., 3.0 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
acetic acid in toluene 72 h; Ambient temperature;
参考文献
Synthesis, , # 7 p. 705 - 713
反应条件
chloroacetic acid in toluene 3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
chloroacetic acid in toluene 3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
chloroacetic acid in toluene 3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
trifluoroacetic acid 1) toluene, 60 deg C, 15 min 2) 60 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
trifluoroacetic acid 1) toluene, 2) r.t., 1.0 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713