2-丙酮基-5,5-二甲基-2-氧代-1,3,2-二氧杂磷杂环己烷合成路线 (共 17 条)
反应条件
chloroacetic acid in toluene 3 h; Ambient temperaturevarious aminals, other 2-oxopropylphosphonate; other α-halo acid, different temperatures and times; Mechanism;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
1: 31 percent / piperidine, acetic acid / benzene / 6.5 h / Heating 2: 45 percent / toluene / 5 h / Heating View Scheme
参考文献
Sakoda; Kamikawaji; Seto
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 9 p. 2362 - 2369
反应条件
chloroacetic acid in toluene 3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Synthesis, , # 7 p. 705 - 713
反应条件
chloroacetic acid in toluene 3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
trifluoroacetic acid 1) toluene, 60 deg C, 15 min 2) 60 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Sakoda; Matsumoto; Seto
Synthesis, 1993 , # 7 p. 705 - 713
反应条件
chloroacetic acid in toluene 3 h; Ambient temperature; Yield given. Title compound not separated from byproducts;
参考文献
Synthesis, , # 7 p. 705 - 713
反应条件
trifluoroacetic acid 1) toluene, 60 deg C, 15 min 2) 60 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Synthesis, , # 7 p. 705 - 713