1-(3,5-二氯-2,6-二羟基-4-甲氧基苯基)己烷-1-酮合成路线 （共 3 条）
反应条件
sulfuryl dichloride in methanol; dichloromethane T=20°C;
参考文献
Exegenics Inc.
Patent: US6828350 B1, 2004 ;
Location in patent: Page/Page column 19 ;
反应条件
1: 58 percent / AlCl3 / CH2Cl2 / 3 h / 20 °C 2: 93 percent / SO2Cl2 / ethanol; CHCl3 / 1 h / 20 °C View Scheme
参考文献
Gokan, Naomi; Kikuchi, Haruhisa; Nakamura, Koji; Oshima, Yoshiteru; Hosaka, Kohei; Kubohara, Yuzuru
Biochemical Pharmacology, 2005 , vol. 70, # 5 p. 676 - 685
反应条件
1: 58 percent / AlCl3 / CH2Cl2 / 3 h / 20 °C 2: 93 percent / SO2Cl2 / ethanol; CHCl3 / 1 h / 20 °C View Scheme
参考文献
Gokan, Naomi; Kikuchi, Haruhisa; Nakamura, Koji; Oshima, Yoshiteru; Hosaka, Kohei; Kubohara, Yuzuru
Biochemical Pharmacology, 2005 , vol. 70, # 5 p. 676 - 685
