5-碘-2-甲基-4(3H)-嘧啶酮合成路线 （共 3 条）
反应条件
iodine in nitric acid T=80°C; 6 h;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Watanabe, Ryo; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2719 - 2724
反应条件
trichlorophosphate Heating;
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Watanabe, Ryo; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2719 - 2724
反应条件
1: 82 percent / POCl3 / Heating
2: 77 percent / Pd(PPh3)2Cl2, CuI, Et3N / 12 h / 80 °C
3: 73 percent / NaOEt, H2S / ethanol / 1.5 h / Heating
View Scheme
参考文献
Sakamoto, Takao; Kondo, Yoshinori; Watanabe, Ryo; Yamanaka, Hiroshi
Chemical & Pharmaceutical Bulletin, 1986 , vol. 34, # 7 p. 2719 - 2724
