4-(叔丁氧羰基氨基甲基)吡啶合成路线 （共 6 条）
反应条件
triethylamine in tetrahydrofuran T=20°C; Acylation;
参考文献
Huang, Xuefei; Borhan, Babak; Rickman, Barry H.; Nakanishi, Koji; Berova, Nina
Chemistry - A European Journal, 2000 , vol. 6, # 2 p. 216 - 224
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=0 - 20°C; 15 h;
参考文献
Caddick, Stephen; Judd, Duncan B.; Lewis, Alexandra K. De K.; Reich, Melanie T.; Williams, Meredith R. V.
Tetrahedron, 2003 , vol. 59, # 29 p. 5417 - 5423
参考文献
US5914319 A1, ;
US 5914319 A
反应条件
triethylamine in 1,4-dioxane; water 30 h; Ambient temperature;
参考文献
Brana, Miguel F.; Castellano, Jose M.; Rodriguez, Maria L. Lopez; Galvez, Magdalena; Amil, Manuel R.; Rubio, Enrique
Journal of Heterocyclic Chemistry, 1987 , vol. 24, p. 369 - 371
反应条件
1: 82 percent / m-CPBA / CH2Cl2 / 12 h / 20 °C 2: 53 percent / dimethylcarbamyl chloride / CH2Cl2 / 48 h / 20 °C 3: 100 percent / aq. NaOH / ethanol / 24 h / Heating View Scheme
参考文献
Huang, Xuefei; Borhan, Babak; Rickman, Barry H.; Nakanishi, Koji; Berova, Nina
Chemistry - A European Journal, 2000 , vol. 6, # 2 p. 216 - 224
反应条件
1: 80 percent / mCPBA / CH2Cl2 / 12 h / 20 °C 2: 53 percent / (CH3)2NCOCl / CH2Cl2 / 48 h / 20 °C View Scheme
参考文献
Huang, Xuefei; Borhan, Babak; Rickman, Barry H.; Nakanishi, Koji; Berova, Nina
Chemistry - A European Journal, 2000 , vol. 6, # 2 p. 216 - 224
