反应条件
1: di-isopropylamine, BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 1 h; 2.) room temp. 1 h
2: 2.) caesium fluoride / 1.) THF, -78 deg C, 5 h, room temp., 5 h; 2.) DMF, room temp., 20 h
3: 95 percent / 10M HCl / tetrahydrofuran / 24 h / Ambient temperature
View Scheme
参考文献
Katritzky, Alan R.; Kuzmierkiewicz, Wojciech
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 819 - 824
