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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
111123-03-6
合成路线
(共 7 条)
111123-03-6
→
反应条件
875-30-9
1,3-二甲基吲哚
+
59045-53-3
反应条件
tetrafluoroboric acid; diethyl ether in acetonitrile Yield given;
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
111123-03-6
→
反应条件
69622-35-1
反应条件
1: tetrafluoroboric acid/ether complex / acetonitrile 2: 90 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature 3: 100 percent / HgO, 35percent aq. tetrafluoroboric acid / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
111123-03-6
→
反应条件
60884-08-4
反应条件
1: tetrafluoroboric acid/ether complex / acetonitrile 2: 60 percent / pyridine / acetonitrile / 7 h / 50 °C 3: HgO, 35percent aq. tetrafluoroboric acid / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria
Synthesis, 1987 , # 3 p. 311 - 314
111123-03-6
→
反应条件
111122-89-5
反应条件
Multi-step reaction with 2 steps 1: tetrafluoroboric acid/ether complex / acetonitrile2: 60 percent / pyridine / acetonitrile / 7 h / 50 °C
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria Synthesis, 1987 , # 3 p. 311 - 314
111123-03-6
→
反应条件
111122-92-0
反应条件
Multi-step reaction with 2 steps 1: tetrafluoroboric acid/ether complex / acetonitrile2: 55 percent / pyridine / acetonitrile / 120 h / Ambient temperature
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria Synthesis, 1987 , # 3 p. 311 - 314
111123-03-6
→
反应条件
111122-97-5
反应条件
Multi-step reaction with 2 steps 1: tetrafluoroboric acid/ether complex / acetonitrile2: 90 percent / pyridine / acetonitrile / 0.5 h / Ambient temperature
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria Synthesis, 1987 , # 3 p. 311 - 314
111123-03-6
→
反应条件
111123-04-7
反应条件
Multi-step reaction with 2 steps 1: tetrafluoroboric acid/ether complex / acetonitrile2: 70 percent / pyridine / acetonitrile / 5 h / Ambient temperature
参考文献
Cadamuro, Silvano; Degani, Iacopo; Fochi, Rita; Gatti, Antonella; Regondi, Valeria Synthesis, 1987 , # 3 p. 311 - 314