N-(1H-苯并三唑-1-基甲基)苯酰胺合成路线 (共 18 条)
反应条件
in toluene 24 h; Heating;
参考文献
Katritzky, Alan R.; Drewniak, Malgorzata
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2339 - 2344
反应条件
N-ethyl-N,N-diisopropylamine in acetonitrile T=60°C; 5.5 h; Sealed tube; Overall yield = 98 percent;
参考文献
Pazdzierniok-Holewa, Agnieszka; Adamek, Jakub; Mazurkiewicz, Roman; Zielinska, Katarzyna
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 1-3 p. 205 - 212
反应条件
1: base 2: N-ethyl-N,N-diisopropylamine / acetonitrile / 5.5 h / 60 °C / |Sealed tube View Scheme
参考文献
Pazdzierniok-Holewa, Agnieszka; Adamek, Jakub; Mazurkiewicz, Roman; Zielinska, Katarzyna
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 1-3 p. 205 - 212
参考文献
Pearson; Stevens
Synthesis, 1994 , # 9 p. 904 - 906
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 0.5 h; Heating;
参考文献
Katritzky, Alan R.; Drewniak, Malgorzata
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2339 - 2344
反应条件
sodium ethanolate Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 57, # 2 p. 547 - 549
反应条件
boron trifluoride diethyl etherate in trichloroethane, 1,1,2-
24 h; Heating;
参考文献
Katritzky, Alan R.; Ignatchenko, Alexey V.; Lang, Hengyuan
Journal of Organic Chemistry, 1995 , vol. 60, # 13 p. 4002 - 4005
反应条件
1: N-(1H-benzotriazol-1-ylmethyl)benzamide With zinc dibromide in dichloromethane
Elimination; 2 h; Heating;
2: 1-morpholino-cyclohexene With zinc dibromide in dichloromethane
amidoalkylation; 20 h; Heating;
参考文献
Katritzky, Alan R.; Fang, Yunfeng; Silina, Alina
Journal of Organic Chemistry, 1999 , vol. 64, # 20 p. 7622 - 7624
反应条件
in tetrahydrofuran
T=25°C;
参考文献
Katritzky, Alan R.; Harris, Philip A.
Tetrahedron, 1990 , vol. 46, # 3 p. 987 - 996
反应条件
in tetrahydrofuran
T=25°C;
参考文献
Katritzky, Alan R.; Harris, Philip A.
Tetrahedron, 1990 , vol. 46, # 3 p. 987 - 996