Zn in tetrahydrofuran mixture of Mo-compound, Zn metal dust and trimethylphosphine was stirred at room temp. in THF under Ar for 36 h; filtn., the ppt. was treated with acetone, filtn., the filtrate was layered with hexane, crystn. after several days of standing;
参考文献
Cotton, F. Albert; Shang, Maoyu; Sun, Zhong Sheng
Journal of the American Chemical Society, 1991 , vol. 113, # 18 p. 6917 - 6922
in dichloromethane byproducts: CO; Stirring of mixt. at room temp. for 2 h, during this period, one molar equiv. of CO to TBAFe evolved; Evapn. in vac., chromy. (silica gel, pentane).;
参考文献
Itoh, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 10 p. 2965 - 2977
Popov, A. M.; Egorova, M. B.
Journal of General Chemistry USSR (English Translation), 1988 , vol. 58, p. 1493 - 1494
Zhurnal Obshchei Khimii, 1988 , vol. 58, p. 1673 - 1674
in toluene Kinetics; no ion exchange between solid KCl and Bu4NBr in toluene (50-105°C);
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 37, p. 239 - 241
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 37, p. 314 - 316
