反应条件
1: sodium tetrahydroborate / benzene / 3.5 h / 0 - 20 °C / Inert atmosphere
2: 2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride / benzene / Inert atmosphere; Reflux
3: triethylamine; p-toluenesulfonyl chloride / dichloromethane / 24 h / 0 - 20 °C / Inert atmosphere
View Scheme
参考文献
Shibatomi, Kazutaka; Kobayashi, Fumito; Narayama, Akira; Fujisawa, Ikuhide; Iwasa, Seiji
Chemical Communications, 2012 , vol. 48, # 3 p. 413 - 415
