N-(2,4-二甲基戊烷-3-亚基)羟胺合成路线 (共 14 条)
反应条件
hydroxylamine hydrochloride; sodium acetate; sodium chloride in ethanol 48 h; Heating;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2073 - 2078
反应条件
nitrosyl chloride Irradiation;
参考文献
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 260, p. 4514 - 4517
反应条件
in 1,2,3,4-tetrahydro-naphthalene T=149.84°C; 264 h; KineticsProduct distribution; Further Variations:Solvents;
参考文献
Organic and Biomolecular Chemistry, , vol. 2, # 3 p. 415 - 420
反应条件
aluminum oxide T=350 - 360°C;
参考文献
Mailhe; de Godon
Bulletin de la Societe Chimique de France, 1918 , vol. <4> 23, p. 18
Chem. Zentralbl., 1918 , vol. 89, # I p. 610
反应条件
T=350 - 360°C; Produkt5:Ammoniak;
参考文献
Mailhe; de Godon
Bulletin de la Societe Chimique de France, 1918 , vol. <4> 23, p. 18
Chem. Zentralbl., 1918 , vol. 89, # I p. 610
反应条件
CC-2; water in acetonitrile T=20°C; 0.416667 h;
参考文献
Gupta, Arvind K.; Acharya, Jyotiranjan; Pardasani, Deepak; Dubey, Devendra K.
Journal of Chemical Research, 2007 , # 7 p. 411 - 414
反应条件
1: 2,4-dimethylpentane-3-one oxime With potassium hydroxide in dimethyl sulfoxide; pentane T=110 - 115°C; Metallation; 0.0833333 h; 2: acetylene in dimethyl sulfoxide; pentane T=70°C; Addition; Vinylation; P=12160 Torr; 0.5 h;
参考文献
Trofimov, Boris A.; Al'bina, Mikhaleva I.; Vasil'tsov, Alexander M.; Schmidt, Elena Yu.; Tarasova, Ol'ga A.; Morozova, Ludmila V.; Sobenina, Lubov' N.; Preiss, Thomas; Henkelmann, Jochem
Synthesis, 2000 , # 8 p. 1125 - 1132
反应条件
potassium hydroxide in dimethyl sulfoxide T=20 - 35°C; Etherification; Alkylation; Hydrolysis; 2.5 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 35, # 11 p. 1581 - 1586
反应条件
bromo-dimethylsulfonium bromide T=80°C; Beckmann rearrangement; 2.5 h; Ionic liquid;
参考文献
Yadav, Lal Dhar S.; Garima; Srivastava, Vishnu P.
Tetrahedron Letters, 2010 , vol. 51, # 4 p. 739 - 743
反应条件
2,4,6-trichloro-1,3,5-triazine; zinc(II) chloride in acetonitrile
Beckmann rearrangement; 1 h; Heating;
参考文献
Furuya, Yoshiro; Ishihara, Kazuaki; Yamamoto, Hisashi
Journal of the American Chemical Society, 2005 , vol. 127, # 32 p. 11240 - 11241