反-4-Boc-氨基环己醇合成路线 （共 13 条）
反应条件
1: With 1H-imidazole; iodine; triphenylphosphine in dichloromethane
T=20°C; Inert atmosphere;
2: With 1,8-diazabicyclo[5.4.0]undec-7-ene in tetrahydrofuran
18 h; Reflux;
参考文献
Alvarez-Perez, Monica; Marco-Contelles, Jose
Synthesis, 2009 , # 21 p. 3649 - 3653
反应条件
1H-imidazole; iodine; triphenylphosphine in dichloromethane
T=20°C; Inert atmosphere;
参考文献
Alvarez-Perez, Monica; Marco-Contelles, Jose
Synthesis, 2009 , # 21 p. 3649 - 3653
反应条件
1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 2 h / 0 °C
2: hydrogenchloride / 1,4-dioxane / 20 h / 0 °C
View Scheme
参考文献
Kawanishi, Eiji; Matsumura, Takehiko
Patent: US2011/160206 A1, 2011 ;
