(9CI)-4-甲基嘧啶并[1,2-a]苯并咪唑-2-胺合成路线 (共 3 条)
反应条件
hydrogenchloride; bis(acetylacetonate)nickel(II) 1.) 130 deg C, 30 min, 2.) reflux, 2.5 h; Yield given. Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 2 p. 418
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 2 p. 458 - 459
反应条件
hydrogenchloride 1) DMF, 130 - 140 deg C, 45 min, 2) 2 h, reflux; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2354 - 2362
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2600 - 2608
反应条件
hydrogenchloride; bis(acetylacetonate)nickel(II) 1) 130 - 140 deg C, 40 min, 2) 2.5 h, reflux; Yield given. Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2354 - 2362
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2600 - 2608