1-叔丁基-2,2,4,4,4-五(二甲氨基)-2Λ5,4Λ5-连二(磷氮基化合物)合成路线 (共 5 条)
反应条件
Yield given. Multistep reaction;
参考文献
Angewandte Chemie, , vol. 99, # 11 p. 1212 - 1214
反应条件
in xylene T=70°C; 5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Liebigs Annales, , # 7 p. 1055 - 1081
反应条件
CF3O3S(1-)*C83H71O2S(1+) in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Piccinini, Alessandro; Kavanagh, Sarah A.; Connon, Stephen J.
Chemical Communications, 2012 , vol. 48, # 63 p. 7814 - 7816
反应条件
CF3O3S(1-)*C83H71O2S(1+) in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; enantioselective reaction;
参考文献
Piccinini, Alessandro; Kavanagh, Sarah A.; Connon, Stephen J.
Chemical Communications, 2012 , vol. 48, # 63 p. 7814 - 7816
反应条件
CF3O3S(1-)*C83H71O2S(1+) in tetrahydrofuran T=-78 - 20°C; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Piccinini, Alessandro; Kavanagh, Sarah A.; Connon, Stephen J.
Chemical Communications, 2012 , vol. 48, # 63 p. 7814 - 7816