(Z)-2-甲氧基-5-(2-(7-甲氧基-苯并[d][1,3]二氧代-5-基)乙烯基)苯酚合成路线 （共 14 条）
反应条件
1.1: tetrabutylammomium bromide; potassium hydroxide / 0.67 h / 100 °C 2.1: pyridine; ozone / methanol; chloroform / -15 - 0 °C 3.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere 3.2: 10 h / 20 °C / Inert atmosphere 4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Journal of Natural Products, , vol. 73, # 11 p. 1796 - 1802
反应条件
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.5 h / -78 °C / Inert atmosphere 1.2: 10 h / 20 °C / Inert atmosphere 2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Journal of Natural Products, , vol. 73, # 11 p. 1796 - 1802
反应条件
in 1,4-dioxane; water 5 h; Irradiationequilibrium;
参考文献
Canadian Journal of Chemistry, , vol. 65, # 10 p. 2390 - 2396
反应条件
n-butyllithium 1) THF, -50 deg C to RT, 20 min, 2) THF, RT, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Canadian Journal of Chemistry, , vol. 65, # 10 p. 2390 - 2396
