反应条件
Multi-step reaction with 4 steps 1: 87 percent / diethyl ether; pyridine / 0 deg C, 2 h. then 22 deg C, 24 h.2: 77 percent / triphenylphosphine, diethylazodicarboxylate / tetrahydrofuran / 22 °C3: N-methylmorpholine N-oxide hydrate, osmium tetroxide / H2O; 2-methyl-propan-2-ol; acetone / 24 h / 22 °C4: 79 percent / hydrazine hydrate / ethanol / 2 h / 60 °C
参考文献
Mulzer; Brand Tetrahedron, 1986 , vol. 42, # 21 p. 5961 - 5968