2,4-二硝基苯基-2-氟-2-脱氧-beta-d-吡喃葡萄糖苷合成路线 (共 4 条)
反应条件
methanol; acetyl chloride T=0 - 20°C; Deacetylation;
参考文献
Journal of the American Chemical Society, , vol. 122, # 7 p. 1270 - 1277
反应条件
1.1: 1,4-diazabicyclo[2.2.2]octane / dimethylformamide / 20 °C 1.2: dimethylformamide / 1.5 h / 20 °C 2.1: 45 percent / acetyl chloride; methanol / 0 - 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 122, # 7 p. 1270 - 1277
反应条件
1.1: 1,4-diazabicyclo[2.2.2]octane / dimethylformamide / 20 °C 1.2: dimethylformamide / 1.5 h / 20 °C 2.1: 45 percent / acetyl chloride; methanol / 0 - 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 122, # 7 p. 1270 - 1277
反应条件
1: 2.) DABCO / 1.) hydrolysis 2: NaOMe / methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, # 24 p. 7530 - 7531