1: in tetrahydrofuran
T=-78°C; 0.666667 h;
2: With sodium tetrahydroborate in tetrahydrofuran; ethanol
T=-78 - 20°C; 1 h; Further stages. Title compound not separated from byproducts.;
参考文献
Vorontsova; Zhuravsky; Sergeeva; Vorontsov; Starikova; Rozenberg
Russian Chemical Bulletin, 2007 , vol. 56, # 11 p. 2225 - 2231