Hermans, J. P. G.; Poot, L.; Kloosterman, M.; Marel, G. A. van der; Boeckel, C. A. A. van; et al.
Recueil des Travaux Chimiques des Pays-Bas, 1987 , vol. 106, # 9 p. 498 - 504
Multi-step reaction with 3 steps 1: acetic acid; H2O / 4 h / 50 °C2: pyridine / Ambient temperature3: 86 percent / 1.) sodium hydride / dimethylformamide / 1.) 0 deg C 30 min; 2.) 0 deg C 30 min; 3.) room temperature overnight
参考文献
Hermans, J. P. G.; Poot, L.; Kloosterman, M.; Marel, G. A. van der; Boeckel, C. A. A. van; et al. Recueil des Travaux Chimiques des Pays-Bas, 1987 , vol. 106, # 9 p. 498 - 504
Multi-step reaction with 4 steps 1: 80 percent / sodium borohydride / tetrahydrofuran / 55 °C / 2.) methanol 45 min and 1h2: acetic acid; H2O / 4 h / 50 °C3: pyridine / Ambient temperature4: 86 percent / 1.) sodium hydride / dimethylformamide / 1.) 0 deg C 30 min; 2.) 0 deg C 30 min; 3.) room temperature overnight
参考文献
Hermans, J. P. G.; Poot, L.; Kloosterman, M.; Marel, G. A. van der; Boeckel, C. A. A. van; et al. Recueil des Travaux Chimiques des Pays-Bas, 1987 , vol. 106, # 9 p. 498 - 504
Multi-step reaction with 5 steps 1: LiAlH4, tetrakis(triphenylphosphine)palladium / dioxane / 0.25 h2: 80 percent / sodium borohydride / tetrahydrofuran / 55 °C / 2.) methanol 45 min and 1h3: acetic acid; H2O / 4 h / 50 °C4: pyridine / Ambient temperature5: 86 percent / 1.) sodium hydride / dimethylformamide / 1.) 0 deg C 30 min; 2.) 0 deg C 30 min; 3.) room temperature overnight
参考文献
Hermans, J. P. G.; Poot, L.; Kloosterman, M.; Marel, G. A. van der; Boeckel, C. A. A. van; et al. Recueil des Travaux Chimiques des Pays-Bas, 1987 , vol. 106, # 9 p. 498 - 504
