N-甲基-N-甲氧基胺盐酸盐合成路线 (共 166 条)
参考文献
Kreutzkamp,N.; Messinger,P.
Chemische Berichte, 1967 , vol. 100, p. 3463 - 3465
参考文献
Jones
American Chemical Journal, 1898 , vol. 20, p. 25
反应条件
T=298°C; rearrangement of N-oxide to O-alkyl hydroxylamines , ΔH, ΔS, ΔG; Thermodynamic data;
参考文献
Goldblum, Amiram; Loew, Gilda H.
Journal of the American Chemical Society, 1985 , vol. 107, # 14 p. 4265 - 4272
反应条件
pyridine; water; methyllithium in diethyl ether; hexane
参考文献
Beak, Peter; Basha, Anwer; Kokko, Bruce; Loo, DeKai
Journal of the American Chemical Society, 1986 , vol. 108, # 19 p. 6016 - 6023
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kokko, Bruce J.; Beak, Peter
Tetrahedron Letters, 1983 , vol. 24, # 6 p. 561 - 564
反应条件
in tetrahydrofuran
T=-78°C;
参考文献
Murphy, John A.; Commeureuc, Aurelien G. J.; Snaddon, Thomas N.; McGuire, Thomas M.; Khan, Tanweer A.; Hisler, Kevin; Dewis, Mark L.; Carling, Robert
Organic Letters, 2005 , vol. 7, # 7 p. 1427 - 1429
反应条件
isopropylmagnesium chloride in tetrahydrofuran
T=-15 - 0°C; 1 h; Inert atmosphere;
参考文献
Cusso, Olaf; Garcia-Bosch, Isaac; Ribas, Xavi; Lloret-Fillol, Julio; Costas, Miquel
Journal of the American Chemical Society, 2013 , vol. 135, # 39 p. 14871 - 14878
参考文献
Persson, Tobias; Nielsen, John
Organic Letters, 2006 , vol. 8, # 15 p. 3219 - 3222
反应条件
1: With triethylamine
T=0°C;
2: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; triethylamine
参考文献
Falkiewicz; Wisniowski; Kolodziejczyk; Wisniewski
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 4-7 p. 1393 - 1397
反应条件
1: 3-phenylpropionic acid With N-ethyl-N,N-diisopropylamine; [bis(2-methoxyethyl)amino]-sulfur trifluoride in N,N-dimethyl-formamide
T=0°C; 0.25 h;
2: N,O-dimethyl-hydroxylamine in N,N-dimethyl-formamide
T=0 - 20°C; 8 h; Further stages.;
参考文献
Tunoori, Ashok Rao; White, Jonathan M.; Georg, Gunda I.
Organic Letters, 2000 , vol. 2, # 25 p. 4091 - 4093