in tetrahydrofuran (C4H9)3SnCH2CCH is added to a soln. of C2H5MgBr in THF; stirring at 60-70°C for 0.75 h; addn. of (H3C)3SiBr; stirring at 70°C for2 h;; distn.; elem. anal.;
参考文献
Bogoradovskii, E. T.; Girbasova, N. V.; Zavgorodnii, V. S.; Petrov, A. A.
Journal of General Chemistry USSR (English Translation), 1986 , vol. 56, p. 2482 - 2483
Zhurnal Obshchei Khimii, 1986 , vol. 56, p. 2801 - 2802
Bogoradovskii, E. T.; Girbasova, N. V.; Zavgorodnii, V. S.; Petrov, A. A.
J. Gen. Chem. USSR (Engl. Transl.), 1986 , vol. 56, # 12 p. 2801 - 2802,2482 - 2483
