1-苯基-2-(m-羟基苯基)乙炔合成路线 (共 4 条)
反应条件
potassium carbonate; copper(l) chloride in methanol; acetonitrile
T=25 - 30°C; Sonogashira Cross-Coupling; 8 h; Inert atmosphereIrradiation;
参考文献
Sagadevan, Arunachalam; Hwang, Kuo Chu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 18 p. 3421 - 3427
反应条件
C16H28Cl2NPPd; caesium carbonate in acetonitrile
T=80°C; Sonogashira Cross-Coupling; 4 h; Inert atmosphere;
参考文献
Pu, Xiaotao; Li, Hongbo; Colacot, Thomas J.
Journal of Organic Chemistry, 2013 , vol. 78, # 2 p. 568 - 581
反应条件
triethylamine; palladium complex immobilised on silica gel in various solvent(s)
T=70°C; Sonogashira coupling; 12 h;
参考文献
Bandini, Marco; Luque, Rafael; Budarin, Vitaly; Macquarrie, Duncan J.
Tetrahedron, 2005 , vol. 61, # 41 p. 9860 - 9868
反应条件
1,4-diaza-bicyclo[2.2.2]octane
T=130°C; Sonogashira coupling; 60 h;
参考文献
Luque, Rafael; MacQuarrie, Duncan J.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 8 p. 1627 - 1632