2-(2-叠氮基乙基)-1,3-二氧戊环合成路线 (共 5 条)
反应条件
sodium azide in dimethyl sulfoxide T=20°C; 14 h;
参考文献
Diez-Gonzalez, Silvia; Escudero-Adan, Eduardo C.; Benet-Buchholz, Jordi; Stevens, Edwin D.; Slawin, Alexandra M. Z.; Nolan, Steven P.
Dalton Transactions, 2010 , vol. 39, # 32 p. 7595 - 7606
参考文献
Rossy, Cybille; Majimel, Jerome; Delapierre, Mona Treguer; Fouquet, Eric; Felpin, Francois-Xavier
Journal of Organometallic Chemistry, 2014 , vol. 755, p. 78 - 85
参考文献
Carboni, B.; Vaultier, M.; Carrie, R.
Tetrahedron, 1987 , vol. 43, # 8 p. 1799 - 1810
反应条件
1: 1.) Ph3P, 2.) H2O / 1) THF, 3 h, below 40 deg C, 20 deg C (1 h); 2) 1 h, 20 deg C 2: 57 percent / triethylamine / 4.5 h / 75 °C View Scheme
参考文献
Gribble, Gordon W.; Switzer, Frank L.
Synthetic Communications, 1987 , vol. 17, # 4 p. 377 - 384
反应条件
hydrogen; interlamellar montmorillonitediphenyl phosphine palladium(II) in ethanol 0.416667 h; Ambient temperature;
参考文献
Sharma, G. V. M.; Chandrasekhar, S.
Synthetic Communications, 1989 , vol. 19, # 19 p. 3289 - 3294