反应条件
1: (6-bromo-1,3,4,5-tetrahydro-benzo[cd]indol-4-yl)-dipropyl-amine With tert.-butyl lithium; potassium hydride in diethyl ether; pentane
T=-78 - -40°C;
2: trimethylsilyl isocyanate in diethyl ether; pentane
T=-78 - -10°C;
参考文献
Wheeler, William J.; Swanson, Steven P.; Varie, David L.; O'Bannon, Douglas D.
Journal of Labelled Compounds and Radiopharmaceuticals, 2005 , vol. 48, # 2 p. 139 - 148